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目的:以复方金果榄汤剂的有效部位提取物制备金山咽速康喷雾剂,拟订质量控制方法。方法:取金果榄、山豆根药材总生物碱提取物,溶解,过滤,调节pH,分装于喷雾剂容器中,即得;采用TLC法对金果榄、山豆根进行鉴别;采用HPLC法对盐酸巴马汀和氧化苦参碱进行含量测定。结果:金果榄、山豆根TLC鉴别实验的供试品色谱中,在与对照品色谱相应的位置上,显相同颜色的斑点;HPLC法测定喷雾剂中盐酸巴马汀的含量为0.063g.L-1,氧化苦参碱含量为0.19g.L-1。结论:本制剂使用方便,质量可控。
OBJECTIVE: To prepare Jinshan yasukangkang aerosol spray from the effective part extract of compound Jinguolu decoction and to develop a quality control method. Methods: The total alkaloid extract of Radix Ranunculus and Radix et Rhizoma Radix was dissolved, filtered, pH was adjusted and dispensed in a spray container. The TLC and HPLC were used to identify Radix Camellia oleifera and Radix et Rhizoma. HPLC determination of palmatine hydrochloride and oxymatrine. Results: The results showed that the same color spots were observed in the chromatogram of the test fruits of TLC. The content of palmatine hydrochloride in the spray was 0.063gL -1, oxymatrine content of 0.19gL-1. Conclusion: The preparation is easy to use and its quality is controllable.