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The crystal of the title compound (C_ 11H_ 11NOS_2, M_r =237.33) has been prepared and determined by X-ray single crystal diffraction. The crystal is monoclinic, space group P2_1/c with parameters : a=5.484 (1), b=7.793(2), c=28.295(6), β=90.277(4)°, V=1209.2(5)3, Z=4, D_c=1.034 g/cm3, μ(MoKα)= 0.413 mm -1, F(000)=496, the final R=0.0390 and wR=0.1051 for 1500 observed reflections with I>2σ(I). The X-ray analysis result shows that the orientation of methylsulfinyl and phenyl is the cis and confirms the E-stereochemistry of the title compound.
The crystal of the title compound (C_11H_11NOS_2, M_r = 237.33) has been prepared and determined by X-ray single crystal diffraction. The crystal is monoclinic, space group P2_1 / c with parameters: a = 5.484 7.793 (2), c = 28.295 6, β = 90.277 (4) °, V = 1209.2 (5) 3, Z = 4, D_c = 1.034 g / cm3, μ (MoKα) = 0.413 mm -1 , The final R = 0.0390 and wR = 0.1051 for 1500 observed reflections with I> 2σ (I). The X-ray analysis result shows that the orientation of methylsulfinyl and phenyl is the cis and the confirms the E -stereochemistry of the title compound.