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安宫牛黄丸是传统名贵中成药,具有清热解毒、镇惊开窍的作用。临床上用于温邪里热,邪入心包引起的高热惊厥,神昏谵语等病症,在国内外市场享有盛誉。《中国药典》一九九○年版也予收载,但只对其挥发性成分麝香酮用 GC 法进行了定性鉴别。本文利用二阶程序升温气相色谱法对安宫牛黄丸中的麝香与冰片进行定性鉴别。1 仪器与试剂1.1 仪器 SQ—203GC 接 A4500色谱数据处理机
Angong Niuhuang Pill is a traditional Chinese proprietary Chinese medicine that has the functions of clearing away heat and detoxifying the stomach and relieving it. Clinically used in heat evil heat, evil caused by high fever convulsions caused by constipation, God faint language and other illnesses, reputation in the domestic and foreign markets. The Chinese Pharmacopoeia (1990 edition) is also included, but only the volatile components of musk ketone were qualitatively identified by the GC method. In this paper, the qualitative identification of the musk and borneol in Angong Niuhuang Pills was conducted by the second-order temperature-programmed gas chromatography. 1 instruments and reagents 1.1 instrument SQ-203GC connected A4500 chromatography data processor