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1引言用毛细管胶束电动色谱(MEKC)对PTC氨基酸分离条件进行研究,建立MEKC分离17种PTC氨基酸的方法。结果表明,在20min内17种PTC氨基酸得到比较满意的分离,方法回收率为95%~103%,在60μmol/L浓度范围内均呈线性,相关系数r>
1 Introduction The separation of PTC amino acids by capillary micellar electrokinetic chromatography (MEKC) was studied to establish a method for the separation of 17 kinds of PTC amino acids by MEKC. The results showed that 17 kinds of PTC amino acids were satisfactorily separated in 20 min, the recoveries were between 95% and 103%, linear in the concentration range of 60 μmol / L, the correlation coefficient r>