以二茂铁为起始原料 ,经多步反应合成了二茂铁二乙酰氯 ,后者与羟胺反应合成了新化合物 1 ,1′-二茂铁二乙酰羟胺 ,以此为配体与氯化稀土反应合成了七种配合物 .通过元素分析 ,红外光谱 ,核磁共振氢谱确定了化合物的组成和结构 Starting from ferrocene, ferrocene diacetyl chloride was synthesized by multi-step reaction, and the latter was reacted with hydroxylamine to synthesize a novel compound 1, 1’-ferrocene diacetylhydroxylamine, which was used as ligand and chloride Seven complexes were synthesized by the reaction of rare earth elements.The composition and structure of the compounds were confirmed by elemental analysis, IR and 1H-NMR