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一、研究用材料及实验内容1. 研究时效温度、时间对组织影响的实验材料合金化学成份列于表1。表1、实验用GH169合金试样的成份(棒材)┏━━━┳━━━━━┳━━━━━┳━━━━┳━━━━━┳━━━━━┳━━━━━┳━━━━━┳━━━━┳━━━━┳━━━━┳━━━━┳━━━━━┳━━━━┳━━━━━┳━━━━┓┃┃┃ _ ┃┃┃┃┃┃┃┃┃┃┃┃┃┃┃┃ C ┃ Ma ┃ Si ┃ S ┃ P ┃ Cr ┃ Ni ┃ Mo ┃ Nb ┃ AI ┃ Ti ┃ B ┃ Cu ┃ Mg ┃ CO ┃┣━━━╋━━━━━╋━━━━━╋━━━━╋━━━━━╋━━━━━╋━━━━━╋━━━━━╋━━━━╋━━━━╋━━━━╋━━━━╋━━━━━╋━━━━╋━━━━━╋━━━━┫┃┃┃┃┃┃┃┃ 520.0 ┃ 2.95 ┃ 5.12 ┃┃ 0.98 ┃┃┃ O.0025 ┃┃┃％┃ 0.046 ┃ 0.03 ┃ 0.10 ┃ 0.002 ┃ 0.004 ┃ 18.74 ┃┃┃┃ 0.49 ┃┃ 0.005 ┃ 0.07 ┃┃ 0.05 ┃┃┃┃┃┃┃┃┃ 521.0 ┃ 2.96 ┃ 5.16 ┃┃ 1.00 ┃┃┃ 0.0048 ┃┃┗━━━┻━━━━━┻━━━━━┻━━━━┻━━━━━┻━━━━━┻━━━━━┻━━━━━┻━━━━┻━━━━┻━━━━┻━━━━┻━━━━━┻━━━━┻━━━━━┻━━━━┛合金经955℃/小时空冷+720℃/8小时,以55℃/小时炉冷至620℃/8小时空冷的完全热处理后,分别在550℃和650℃长期时效,550℃的时效时间选为200、500、1000小时。650℃的时效时间选为100、200、1000小时。2、研究不同Nb、C含量对组织影响的实验材料:合金化学成份列于表2。合金经完全热处理后,在650℃时效5000小时。薄膜试样采用200kV在JEM—2000FX电镜观察。
First, the research materials and experimental content 1. Study of aging temperature, time of the impact of the experimental material alloy chemical composition are shown in Table 1. Table 1, the experimental GH169 alloy sample composition (bar) ┏ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━┳ ━ ┃ C ┃ Ma ┃ Si ┃ S ┃ P ┃ Cr ┃ Ni ┃ Mo ┃ Nb ┃ AI ┃ Ti ┃ B ┃ Cu ┃ Mg ┃ CO ┃┣━━━╋━━━━━╋━━━━━╋━━━━╋━━━━━╋━━━━━╋━━━━━╋━━━━━╋━ ━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━━ 520.0 ┃ 2.95 ┃ 5.12 ┃┃ 0.98 ┃┃┃ O.0025 ┃┃┃% ┃ 0.046 ┃ 0.03 ┃ 0.10 ┃ 0.002 ┃ 0.004 ┃ 18.74 ┃┃┃┃ 0.49 ┃┃ 0.005 ┃ 0.07 ┃┃ 0.05 ┃┃┃┃┃┃┃┃ ┃ 521.0 ┃ 2.96 ┃ 5.16 ┃┃ 1. 00 ┃┃┃ 0.0048 ┃┃┗ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━ ━━┻━━━━┻━━━━┻━━━━┻━━━━┻━━━━━┻━━━━┻━━━━━┻━━━━┛ alloy by 955 ℃ / Hours air cooling +720 ° C / 8 hours, with 55 ° C / hour furnace cooling to 620 ° C / 8 hours air cooling after complete heat treatment, respectively 550 ° C and 650 ° C long-term aging, 550 ° C aging time selected 200,500,1000 hour. 650 ℃ aging time selected as 100,200,1000 hours. 2, the study of different Nb, C content on the impact of experimental materials: alloy chemical composition are shown in Table 2. After the alloy has been completely heat treated, the alloy is aged at 650 ° C for 5000 hours. Film samples were observed using a 200 kV electron microscope at JEM-2000FX.