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A novel compound of 9-[3-oxo-1-(4-bromopheny)-3-phenypropyl]fluorine (3) was synthesized via nucleophilic addition reaction under solvent-free condition. Its structure was determined by IR, 1H NMR, MS, elemental analysis and X-ray diffraction. The crystal of the new compound is of triclinic system, space group P-1 with a=9.7919(16), b=11.0932(18), c=11.2534(19) , α=76.927(3), β=67.452(3), γ=84.895(3)°, V=1099.7(3) 3, Z=2, Dc=1.369 g/cm3, μ=1.886 mm-1, F(000)=464, R=0.0586 and wR=0.1562 for 3145 observed reflections with Ⅰ > 2σ(Ⅰ). π-π Stacking interactions contribute to the stability of the structure.
Its structure was determined by IR, 1 H NMR, MS (CDCl 3) The crystal of the new compound is of triclinic system, space group P-1 with a = 9.7919 (16), b = 11.0932 (18), c = 11.2534 (19) 76.927 (3), β = 67.452 (3), γ = 84.895 (3) °, V = 1099.7 (3) 3, Z = 2, Dc = 1.369 g / cm3, μ = 1.886 mm-1, ) = 464, R = 0.0586 and wR = 0.1562 for 3145 observed reflections with I> 2σ (I). Π-π stacking interactions contribute to the stability of the structure.