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目的:建立益气逐瘀丸的质量控制方法并制定标准。方法:应用显微鉴别法对益气逐瘀丸中黄芪、葛根、三七进行显微鉴别;用薄层色谱法对益气逐瘀丸中黄芪、葛根进行定性鉴别,并以高效液相色谱法对制剂中黄芪甲苷进行含量测定。结果:益气逐瘀丸中黄芪甲苷的平均含量为0.07 mg/g,线性回归方程Y=0.6423X-1.2262,(r=0.9999,n=6),平均回收率为:98.99%,RSD=1.78%。结论:所建立的方法准确可靠,重现性好,可用于益气逐瘀丸的质量标准。
Objective: To establish the quality control method of Yiqi Zhuyu Pills and to set the standard. Methods: The microscopic identification method was used to identify the Astragalus root, Radix Puerariae and Radix notoginseng in Yiqi Zhuyu Pill microscopically. The qualitative identification of Radix Astragali, Radix Puerariae was carried out by TLC, Act on the preparation of Astragaloside content determination. Results: The average content of astragaloside in Yiqi Zhuyu Wan was 0.07 mg / g and the linear regression equation was Y = 0.6423X-1.2262 (r = 0.9999, n = 6) 1.78%. Conclusion: The established method is accurate and reproducible, and can be used for the quality standard of Yiqi Zhuyu Pills.