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本文首次用微波辐射法（ＭｉｃｒｏｗａｖｅＲａｄｉａｔｉｏｎＭｅｔｈｏｄ，简称ＭＲＭ）合成了纯的ＳｒＳ基质和ＳｒＳ∶Ｃｅ３＋，Ｋ＋蓝色荧光化合物，用ＸＲＤ测定了它们的晶体结构，系统考察了不同浓度的Ｃｅ３＋离子对发光性能的影响。实验发现，微波辐射能使Ｃｅ３＋在ＳｒＳ基质晶格中均匀扩散，并能提高激活剂的掺入量，阻止Ｃｅ３＋离子的簇集，延缓Ｃｅ３＋离子对的形成，从而能得到晶相纯、粒度均匀和发光效率高的ＳｒＳ∶Ｃｅ３＋，Ｋ＋蓝色荧光体。
In this paper, pure SrS and SrS: Ce3 +, K + blue fluorescent compounds were synthesized by Microwave Radiation Method (MRM) for the first time. Their crystal structures were determined by XRD. The effects of different concentrations of Ce3 + ions on the luminescent properties influences. It is found that the microwave radiation can make Ce3 + diffuse evenly in the lattice of SrS matrix and can increase the incorporation of activator, prevent the clustering of Ce3 + ions and delay the formation of Ce3 + ion pair, so as to obtain crystal phase pure and uniform particle size And SrS: Ce3 +, K + blue phosphors with high luminous efficiency.