本法采用气相色谱内标定量法,并对影响灵敏度的诸因素,如气体流速、柱温等进行了试验。通过试验了解并证实了响应值、保留值、比值、分离度及柱温相互间的关系与色谱理论一致,并在此基础上选择最佳色谱操作条件,为获得灵敏度高,重现性好,数据精确可靠的快速的色谱分析法提供实验依据。 This method uses gas chromatography internal standard quantification method, and the sensitivity of the factors such as gas flow rate, column temperature were tested. According to the experiment, we know and confirm the relationship between the response value, retention value, ratio, resolution and column temperature with the chromatographic theory, and select the best chromatographic operating conditions, in order to obtain high sensitivity, good reproducibility, Accurate and reliable data for rapid chromatography provides experimental evidence.