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在現有文献中,关於用以說明電解積铼的各种水糟液的數量數据是非常缺乏的。現在对铼化学的興趣以及铼化物的低廉使我們想到;積铼槽液的詳細資料是有價值的。本文的目的存於对電解析铼作半定量实驗研究,並說明新型的電鍍水槽液。槽液的要求資料是通过研究槽液的pH、槽液的組成与陰極電流密度对電流效率与陰極沉積物外貌的影响的方法而收集的。全部研究結果都已加以綜合。初步研究証明: 硫酸、檸檬酸鹽与柠檬酸按槽液得出最好的效果。由於这一原因詳細的研究只限於这三种槽液。后來為了全面瞭解也曾測定其他提出的水槽液的陰極電流效率。
In the prior literature, there is a great lack of quantitative data on various kinds of water spoilage used to explain rhenium electrolysis. The current interest in rhenium chemistry and the low rhenium compounds reminds us; detailed information on rhenium baths is valuable. The purpose of this paper lies in the semi-quantitative experimental study of rhenium electrowinning and the new plating bath solution. The bath requirements data were collected by studying the effect of bath pH, bath composition, and cathodic current density on current efficiency and cathodic deposit appearance. All the research results have been integrated. Preliminary research shows that: sulfuric acid, citrate and citric acid by the best solution. For this reason a detailed study is limited to these three baths. Later on, for the sake of completeness, the cathode current efficiency of other proposed bath solutions has also been measured.