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公开号:CN103592399A公开日:2014.02.19申请人:上海大学摘要:本发明涉及一种可同时检测人体血清中有机氯农药和合成麝香浓度的方法,通过液液萃取–凝胶渗透色谱柱–硅胶氧化铝柱的化学预处理方法结合气相色谱电子捕获检测(GC–ECD)以及气相色谱–质谱联用(GC–MS)的检测技术来达到测定血清中有机氯农药和合成麝香的目的。本发明属于有机化学物质的物理化学分析测定技术领域。
Publication Number CN103592399A Publication Date: 2014.02.19 Applicant: 上海 大学 Abstract: The present invention relates to a method for simultaneous detection of organochlorine pesticides and synthetic musk in human serum by liquid-liquid extraction and gel permeation chromatography The chemical pretreatment of alumina column combined with gas chromatography-electron capture detection (GC-ECD) and gas chromatography-mass spectrometry (GC-MS) detection technology to achieve the purpose of determination of organochlorine pesticides and synthetic musk in serum. The present invention belongs to the technical field of physicochemical analysis and determination of organic chemicals.