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报道了自行研制的制备高纯同位素~(15)N_2气体的装置和方法。其特点是一次可制备0.5-10L间任何量的~(15)N_2气体。用该装置,以(15NH4)2SO4为原料,得到~(15)N_2气体的产率为96.9%-98.4%,~(15)N_2气体中15NH3和15NO的含量在1μg/L以下,其纯度能满足生物固氮研究的要求。
A device and a method for preparing high purity isotope ~ (15) N 2 gas have been reported. Its characteristic is that it can prepare any amount of ~ (15) N 2 gas between 0.5-10L at a time. The yield of ~ (15) N_2 gas was 96.9% -98.4% with (15NH4) 2SO4 as feedstock, and the content of 15NH3 and 15NO in ~ (15) N_2 gas was less than 1μg / L , Its purity can meet the requirements of biological nitrogen fixation.