论文部分内容阅读
用高效液相色谱法测定血浆中曲尼司特浓度。色谱条件:色谱柱为SpherisorbC_(18)柱;乙腈-0.01mol/L磷酸二氢钾溶液(30:70)为流动相;流速为1.2ml/min;检测波长333nm。线性范围1—60μg/ml;最小检出量为0.5μg,平均回收率为91.4%。
Tranilast concentration in plasma was determined by high performance liquid chromatography. Chromatographic conditions: column SpherisorbC_ (18) column; acetonitrile-0.01mol / L potassium dihydrogen phosphate solution (30:70) as the mobile phase; flow rate of 1.2ml / min; detection wavelength 333nm. The linear range of 1-60μg / ml; the minimum detectable amount of 0.5μg, the average recovery was 91.4%.