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A new two dimensional 8 ring network nickle phosphate Ni 3(PO 4) 2·8H 2O was synthesized hydrothermally and its structure was determined by means of single crystal X ray diffraction. The Ni 3(PO 4) 2·8H 2O crystal crystallizes in the monoclinic system, space group C2/m , with M=128.13, a =0^994 7(2) nm, b =1.321 7(3) nm; c =0.463 6(1) nm; β=104.80(3)°, V =0.589 3(2) nm 3, Z=2, R=0.027 2 and wR =0.057 5. The network structure consists of vertex sharing which results in the formation of undulating 4 ring chains and 8 ring sheets.
A new two dimensional 8 ring network nickle phosphate Ni 3 (PO 4) 2 · 8H 2O was formed hydrothermally and its structure was determined by means of single crystal X ray diffraction. The Ni 3 (PO 4) 2 · 8H 2O crystal crystallizes in the monoclinic system space group C2 / m with M = 128.13, a = 0 ^ 994 7 (2) nm, b = 1.321 7 (3) nm; c = 0.463 6 3) °, V = 0.589 3 (2) nm 3, Z = 2, R = 0.027 2 and wR = 0.057 5. The network structure consists of vertex sharing which results in the formation of undulating 4 ring chains and 8 ring sheets.