本文介绍了具有独特物理、化学性质的金属氧化物、硫化物纳米材料的低温固相合成方法,重点阐述了金属氧化物和硫化物纳米材料的低温固相合成方法的路线、反应类型、常用表征测试方法、光电磁性能研究及低温固相反应机理等方面内容,并列举了各种实例。低温固相合成方法在制备金属氧化物、硫化物纳米材料方面具有操作简便、成本低、污染小等优点,可望用于纳米材料的大规模生产。 In this paper, the low-temperature solid-phase synthesis of metal oxides and sulfide nanomaterials with unique physical and chemical properties is introduced. The routes, reaction types and common characterizations of low temperature solid-phase synthesis of metal oxide and sulfide nanomaterials are mainly described Test methods, the study of photoelectromagnetic properties and low temperature solid-state reaction mechanism and other aspects, and cite a variety of examples. The low temperature solid phase synthesis method has the advantages of simple operation, low cost and small pollution in the preparation of metal oxide and sulfide nanomaterials, and is expected to be used for large-scale production of nanomaterials.