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取代苯甲醛 /苯乙酮、3 0 %的过氧化氢 (2 .2当量 )和硼酸 (5当量 )及微量硫酸在四氢呋喃中 ,于室温 (或 60°C)下反应 ,生成酚 ,2 5例收率 3 0 %~ 97%。过氧化氢/硼酸氧化芳香醛和酮成酚RoyA等@徐林
Substituted benzaldehyde / acetophenone, 30% hydrogen peroxide (2.2 equivalents) and boric acid (5 equivalents) and traces of sulfuric acid in tetrahydrofuran at room temperature (or 60 ° C) to produce phenol, 25 Example yield 30% to 97%. Hydrogen peroxide / boric acid oxidation of aromatic aldehydes and ketones into phenol RoyA @ Xu Lin