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The title compound has been synthesized by the reaction of HgI2 and [(CH3)3- NCH2CH2N(CH3)3]I2 with pH = 7.5 at room temperature, and its crystal structure was determined by single-crystal X-ray diffraction analysis. The title compound crystallizes in monoclinic system, space group P21/c with a = 8.3075(8), b =15.8084(19), c =15.390(2) ?, β = 95.192(4)o, V = 2012.9(4) ?3, Z = 2, Dc = 2.824 g/cm3, F(000) = 1502, C14H39N4O2Hg2I8, Mr = 1711.87, μ(MoKα) = 13.768 mm-1, the final R = 0.0465 and wR = 0.1293 for 3046 observed reflections with I > 2σ (I). The title compound consists of cations ([C8H22N2]2+) and anion (HgI4 ), which are combined by static 2- attracting forces to form the so-called organic-inorganic hybrid material.
The title compound has been synthesized by the reaction of HgI2 and [(CH3) 3-NCH2CH2N (CH3) 3] I2 with pH = 7.5 at room temperature, and its crystal structure was determined by single-crystal X-ray diffraction analysis. title compound crystallizes in monoclinic system, space group P21 / c with a = 8.3075 (8), b = 15.8084 (19), c = 15.390 (2) 3, Z = 2, Dc = 2.824 g / cm3, F (000) = 1502, C14H39N4O2Hg2I8, Mr = 1711.87, μ (MoKα) = 13.768 mm-1, the final R = 0.0465 and wR = 0.1293 for 3046 observed reflections with I> 2σ (I). The title compound consists of cations ([C8H22N2] 2+) and anion (HgI4), which are combined by static 2-attracting forces to form the so-called organic-inorganic hybrid material.