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藜芦反丹参早在《神农本草经》中就已提出,并为历代医家所遵守,迄今,为配伍之大忌。但目前已有将二味合用配于复方散剂中.用来治疗咳嗽、痰喘、胸痹、腹泻等疾病,没有造成不良后果的报告。藜芦配丹参后对丹参中成分含量有何影响,还未见报道。本文采用高效液相法对藜芦配丹参后对丹参酮IA含量影响进行了测定,重现性良好,结果满意。一、仪器与药品仪器高效液相色谱仪Waters 510泵,U6K手动进样器,490紫外检测器,745积分仪。试剂甲醇(色谱纯,浙江),二氯甲烷(分析纯,大连),超净水用新鲜蒸馏水自制。
As early as the “Shen Nong’s Materia Medica”, V. reticulata had been proposed and complied with by successive physicians. So far, it has become a taboo for compatibility. However, there are currently reports that the combination of two flavors is used in compound powders to treat diseases such as cough, expectoration, chest spasm, and diarrhea, with no adverse consequences. What effect does the vermilion and Salvia miltiorrhiza have on the content of salvia miltiorrhiza haven’t been reported. In this paper, the effect of Veratrum and Salvia Miltiorrhizae on the content of tanshinone IA was determined by HPLC. The reproducibility was good and the results were satisfactory. First, instruments and pharmaceutical instruments High-performance liquid chromatograph Waters 510 pump, U6K manual sampler, 490 UV detector, 745 integrator. Reagents Methanol (Chromatographically Pure, Zhejiang), Dichloromethane (Analytical Pure, Dalian), Ultra Purified Water Home Made with Fresh Distilled Water.