Facile synthesis of coordination polymer nanocubes and their conversion into mesoporous single cryst

来源 :Chinese Chemical Letters | 被引量 : 0次 | 上传用户:gx2784500
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Mesoporous single crystal-like Y_2O_3 nanocubes have been prepared through a coordination-based selfassembly process.Firstly,a uniform nanocube-Iike Y-lysine precursor was simply prepared with hydrothermal treatment.After the simple thermal treatment process,nanocube-shaped yttrium oxides with the morphology inherited from the Y-lysine precursor were successfully prepared.The phase,morphology,size and crystalline structure were well characterized by XRD,SEM and TEM.N_2adsorption-desorption demonstrates the mesoporous characteristics of the Y_2O_3 nanocubes,showing a relatively high surface area of 60 m~2/g. Mesoporous single crystal-like Y_2O_3 nanocubes have been prepared through a coordination-based selfassembly process. Firstly, a uniform nanocube-Iike Y-lysine precursor was simply prepared with hydrothermal treatment. After the simple thermal treatment process, nanocube-shaped yttrium oxides with the morphology inherited from the Y-lysine precursor were successfully prepared in the phase, morphology, size and crystalline structure were well characterized by XRD, SEM and TEM. N2adsorption-desorption demonstrates the mesoporous characteristics of the Y_2O_3 nanocubes, showing a relatively high surface area of 60 m ~ 2 / g.
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