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目的:选取临床上常用的30种清热中药,测定微量元素的含量,研究微量元素的含量特征。方法:采用HNO3-HClO4湿法消化,等离子体发射光谱法测定Mg、Ca、Fe、Zn、Mn、Cu、K、Cr、Cd、Pb等10种微量元素的含量。结果:30种清热中药中对人体有益的微量元素含量丰富,大部分清热类中药中K和Ca含量较高,不同药物中元素含量有所差别,清热解毒中药中K、Mg含量明显高于其他中药,清热泻火类中药中Zn、Mn含量明显高于其他中药。方法的回收率在96.8%~107.3%之间,RSD小于3.06%,具有良好的准确度和精密度。结论:清热中药中微量元素的含量具有显著的特征性。
OBJECTIVE: To select the 30 kinds of heat-clearing traditional Chinese medicines commonly used clinically to measure the content of trace elements and to study the content characteristics of trace elements. Methods: The contents of 10 trace elements such as Mg, Ca, Fe, Zn, Mn, Cu, K, Cr, Cd and Pb were determined by wet digestion with HNO3-HClO4 and plasma emission spectrometry. Results: 30 kinds of heat-clearing traditional Chinese medicine in the human body is beneficial to trace elements rich in content, most of the heat-clearing traditional Chinese medicine K and Ca content is higher, different drugs have different elemental content, Qingrejiedu K, Mg content was significantly higher than the other Chinese medicine, heat purging fire class medicine Zn, Mn content was significantly higher than other Chinese medicine. The recoveries of the method ranged from 96.8% to 107.3% with a RSD of less than 3.06%, with good accuracy and precision. Conclusion: The content of trace elements in heat-clearing traditional Chinese medicine has obvious characteristic.