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用电弧炉和电子束悬浮区熔炉法制备了LaB6ZrB2共晶复合材料,并用SEM和TEM方法对其显微组织进行了研究。结果表明,LaB6ZrB2形成纤维状共晶组织,控制凝固条件可得到定向排列的组织,LaB6基体上均匀分布着直径为02~12μm的ZrB2纤维,纤维长度可达100μm以上。对于固液界面为平面生长的试样,其结晶学取向关系为[001]LaB6∥[001]ZrB2,(110)LaB6∥(010)ZrB2。
LaB6ZrB2 eutectic composite was prepared by electric arc furnace and electron beam suspension zone method. The microstructure of LaB6ZrB2 composite was studied by SEM and TEM. The results show that LaB6ZrB2 can form fibrous eutectic structure and control the solidification conditions to obtain the aligned structure. The ZrB2 fiber with the diameter of 02 ~ 12μm is uniformly distributed on the LaB6 matrix, and the fiber length can reach more than 100μm. The crystallographic orientations of [001] LaB6 // [001] ZrB2, (110) LaB6 // (010) ZrB2 for the solid-liquid interface were plane-grown.