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YIN, Shao Hu MA, Sheng Ming JIAO, Ning TAO, Feng Gang a Department of Chemistry, Fudan University, Shanghai 200433, China b State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China 2,3 Allenols were prepared conveniently from the reduction reaction of 2,3 allenoates with DIBAL H (Diisobutylaluminum hydride) in toluene. A dramatic solvent effect was observed for this reaction.
YIN, Shao Hu MA, Sheng Ming JIAO, Ning TAO, Feng Gang a Department of Chemistry, Fudan University, Shanghai 200433, China b State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China 2,3 Allenols were prepared conveniently from the reduction reaction of 2,3 allenoates with DIBAL H (Diisobutylaluminum hydride) in toluene. A dramatic solvent effect was observed for this reaction.