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A new sulfanilamide Schiff-base compound N,N’-(p-phenyl sulfanilamide)-5,6-dimethoxy-pyrimidine-(2-hydroxyl benzene) methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4-(p-amino phenyl sulfanilamide)-5,6-dimethoxy-pyrimidine in an anhydrous ethanol solution.The compound was characterized by elemental analysis,IR spectra,and single-crystal X-ray diffraction.The crystal belongs to the monoclinic system,space group P21/c with a=19.0425(11),b=11.1914(6),c=9.0075(5),β=93.9650(10)°,Z=4,V=1915.01(18)3,Dc=1.437 g/cm3,Mr=414.43,λ(MoKa)=0.71073,μ=2.09 mm-1,F(000)=864,R=0.0385 and wR=0.1224.
A new sulfanilamide Schiff base compound N, N’- (p-phenyl sulfanilamide) -5,6-dimethoxy-pyrimidine- (2-hydroxyl benzene) methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4- (p-amino phenyl sulfanilamide) -5,6-dimethoxy-pyrimidine in an anhydrous ethanol solution. The compound was characterized by elemental analysis, IR spectra, and single-crystal X-ray diffraction. The crystal belongs to the monoclinic system, space group P21 / c with a = 19.0425 (11), b = 11.1914 (6), c = 9.0075 (5) β, β = 93.9650 (10) °, Z = 4, V = 1915.01 (18) 3, Dc = 1.437 g / cm3 , Mr = 414.43, λ (MoKa) = 0.71073, μ = 2.09 mm-1, F (000) = 864, R = 0.0385 and wR = 0.1224.