论文部分内容阅读
文章概述了自行研制的亚纳克级全反射X射线荧光分析(TXRF)装置的结构和性能。该TXRF分析装置系利用本实验室已有的岛津XD-1型衍射仪的X光发生器及Cu靶衍射管作光源,从国外引进一套两次全反射光路组件,配以Si(Li)探测器-多道微机分析系统组装而成。使用与之配套而开发的SPAN/XRFV4.0X射线谱处理软件。实验测试结果表明,对原子序数为16—28诸元素,探测下限(MDL)达0.1ng量级。
The article outlines the structure and performance of a self-developed Yannian-class total reflection X-ray fluorescence analysis (TXRF) device. The TXRF analyzer utilizes a X-ray generator and a Cu target diffracting tube of the existing Shimadzu XD-1 diffractometer in our laboratory as a light source, introduces a set of total reflection optical path components twice from abroad and is provided with Si (Li Detector - Multi-channel computer analysis system assembled. Use the accompanying SPAN / XRFV4.0X ray spectrum processing software developed. Experimental results show that for the 16-28 atomic number elements, the detection limit (MDL) of 0.1ng order of magnitude.