【摘 要】
：
A solvothermal reaction of anhydrous C3N3Cl3 and sodium using cyclohexane as solvent and NiCl2 as catalyst precursor has been carried out to prepare carbon nitr
【机 构】
：
Research Center of Material Science
论文部分内容阅读
A solvothermal reaction of anhydrous C3N3Cl3 and sodium using cyclohexane as solvent and NiCl2 as catalyst precursor has been carried out to prepare carbon nitride nanotubes successfully at 230℃ and 1.8 MPa. The carbon nitride nanotubes were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), electron diffraction (ED), electron energy loss spectrum (EELS) and Raman spectrum. SEM and TEM results indicated that the tubes have a length of 20-30 μm, a uniform outer diameter of about 50-60 nm, an inner diameter of 30-40 nm and are highly ordered assembled as bundles. The EELS measurement indicated that the ratio of N/C was about 1.00. The ED and XRD analyses revealed that the tube may have a new CN crystalline structure. The growth mechanism of nanotubes was discussed.
其他文献
Semiconductor SnO2 nanotube arrays were fabricated by sol-gel method based on highly ordered nanoporous anodic alumina membrane. Their microstructures were char
Adsorption and oxidation of ethylene glycol (EG) on Pt(100) electrode were studied by in situ time- resolved FTIRS (TRFTIRS). The TRFTIR spectra recorded at 0.1
介绍硬X射线调制望远镜(HXMT)探测器能量响应矩阵的计算方法,根据实验室测量数据计算了该条件下的能量响应矩阵;利用该能量响应矩阵由直接解调法解实验室所测放射源能谱,能很
The Sino-Mongolian border areas underwent two important tectonic events during Mesozoic time after late Paleozoic orogeny: a late Triassic to earlier Jurassic c
It is usually difficult to express a family of tri-point transition function (TTF)by a transition matrix as Markov processes with one parameter. In this paper,
介绍了Lie代数的方法,用Lie代数方法分析了静电分析器对束流传输过程的非线性影响,其计算结果分析到三级近似.首先给出了静电分析器的哈密顿函数,然后将哈密顿函数展开为齐次
在实验室内建立了一套宇宙线测试系统(CORTS),并对一个大面积CMS RE1/2 RPC的完整样品进行了系统的测试.结果为RPC的探测效率约85%,时间分辨率为0.87±0.08ns,空间分辨本领为
The unique Bayes linear unbiased estimator (Bayes LUE) of estimable functions is derived for the singular linear model. The superiority of Bayes LUE over ordina
The spectral and polarity dependence of the quantum yield of charge carrier photo-generation was stud-ied by steady-state photocurrent measurement in a single l