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以乙酰丙酮(1)为原料,经电解氧化偶联,Paal-Knorr闭环,Baeyer-Villiger氧化,水解等步骤,合成了一种重要的杂环香料,2,5-二甲基-4-羟基-3(2H)呋喃酮(6)。
An acetylacetone (1) was used as the starting material to synthesize an important heterocyclic aromatic compound by electrochemical oxidative coupling, Paal-Knorr closed-loop, Baeyer-Villiger oxidation and hydrolysis. 2,5-dimethyl- -3 (2H) furanone (6).