用废铁屑作催化剂，Ｈ２Ｏ２作氧化剂，对炼厂汽提后含硫废水进行了除酚试验研究。考察了初始ｐＨ、Ｈ２Ｏ２投加量、废铁屑投加量对酚去除率的影响。对含酚量为３３１．５ｍｇ／Ｌ的废水，将其初始ｐＨ调至７．２，３０％Ｈ２Ｏ２的投加量为７．５ｍＬ／Ｌ，废铁屑的投加量为３～８ｇ／Ｌ，经２ｈ反应后，酚的脱除率可达９９．９％。 Using scrap iron as catalyst and H2O2 as oxidant, the phenol removal experiment was carried out on the sulfur-containing wastewater after the stripping of the refinery. The effects of initial pH, dosage of H2O2 and scrap iron dosage on phenol removal were investigated. For the wastewater with phenol content of 331.5mg / L, the initial pH was adjusted to 7.2, the dosage of 30% H2O2 was 7.5mL / L, the dosage of waste scrap iron was 3 ~ 8g / L , After 2h reaction, phenol removal rate of up to 99.9%.