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A new molecular imprinted electrochemical sensor has been developed for detection of 3,5-Xylyl methylcarbamate(XMC) by combination of Graphene doped Gold nanoparticle.The molecularly imprinted polymers (MIPs) was synthesized on Graphene doped Gold Nanoparticle modified glassy carbon electrode surface by using XMC as template molecular,methyl acrylic acid as functional monomer,and ethylene glycol maleic rosinate acrylate as cross-linker.The electrochemical performance of the imprinted film was studied with respect to its response to hexacyanoferrate(Ⅲ) as a probe and characterized by cyclic voltammetry (CV) and differential pulse voltammetry (DPV).